Ketoprofen in Human Plasma Assay

 

 

 

 

 

Method: LC-MS/MS

Matrix: Human Plasma

Anticoagulant: Sodium EDTA

Storage Temperature: -20 °C

LLOQ: 0.25 ng/mL

ULOQ: 250 ng/mL

Sample Volume: 0.5 mL

Precision & Accuracy:

  • LLOQ QC: 14.8% CV; 8.0% Bias
  • Low QC: 9.8% CV; 2.0% Bias
  • Mid QC: 8.6% CV; 5.7% Bias
  • High QC: 5.1% CV; 0.4% Bias
  • Above Range QC (10x Dilution): 4.1% CV; -12.7% Bias

Stability:

  • Short-Term (Bench-Top): 4.5 hours
  • Long-Term: 71 days at -20 °C
  • Freeze/Thaw Cycles: 3

Method Number: V1656P1