Flurbiprofen in Human Plasma_Potassium K2EDTA

 

 

 

 

Method: LC-MS/MS

Matrix: Human Plasma

Anticoagulant: Potassium K2EDTA

Storage Temperature: -70 °C

LLOQ: 20.0 ng/mL

ULOQ: 9000 ng/mL

Sample Volume: 150 mcL

Precision & Accuracy:

  • LLOQ QC: 4.8% CV; 4.5% Bias
  • Low QC: 6.9% CV; -2.5% Bias
  • Mid QC: 5.9% CV; -2.7% Bias
  • High QC: 4.4% CV; -2.0% Bias
  • High QC (2x Dilution): 3.9% CV; -4.6% Bias
  • Above Range QC (5x Dilution): 5.6% CV; -7.8% Bias

Stability:

  • Short-Term (Bench-Top): 6 hours
  • Long-Term: 81 days at -70 °C
  • Freeze/Thaw Cycles: 4

Method Number: V2379P1